Dongying Daily/Love Dongying News Since the establishment of Shandong High-end Petrochemical Innovation and Entrepreneurship Community, it has given full play to the industrial and location advantages of Dongying Port Economic Development Zone, with industrialization needs as the traction, and the co-governance and sharing of all participating entities as the link , market mechanism as the criterion, focus on promoting the element units to participate in the whole chain production, R&D, incubation and transformation, focusing on building a chemical pilot base, and promoting the seamless connection between patented technology, scientific research results and enterprise needs, so that the application value is high and the market prospect is good. The local transformation of scientific research results has gradually transformed the development momentum of Dongying Port Economic Development Zone into a "dual-core drive" of innovation and investment.
Rendering of the pilot base of Shandong high-end petrochemical innovation and entrepreneurship community On the basis of the establishment of cooperation between colleges and universities, we have conducted many mutual visits and docking with Shandong Petrochemical Institute . In June this year, we had in-depth exchanges with President Xu Chunming on cooperation and co-construction. The next step will be the focus of the two parties Carry out pragmatic cooperation in the fields of polymer composite materials , homogeneous mixture membrane separation, petrochemical catalysts, solid waste recycling, environmental pollution control, fine chemical synthesis and other disciplines to help the transformation and upgrading of the regional chemical industry and the high-quality development of ." said Guo Feng, director of the General Management Department of Shandong Industry Research Institute Zhongke High-end Chemical Industry Technology Research Institute.
At the same time, Shandong Institute of Petrochemical Technology has established a close cooperative relationship with the community in terms of professional setting, discipline construction, talent training, etc., and constantly provides talents and technical support for the construction of the community. , Achievement transformation base, promote the realization of co-construction, sharing, and win-win, and form a chemical reaction of collaborative innovation.
"In order to meet the high-end development needs of the petrochemical and chemical industry, we make full use of the platform of the community to speed up the promotion of the quality of professional talents." said Geng Shulin, deputy director of the technical operation department of the Shandong Chemical Pilot Base. It is understood that by carrying out various forms of online and offline training, learning and exchange activities between enterprises, universities and scientific research institutes, the community promotes the collaboration of industry-university-research institutes, and helps member companies to improve the ability and level of innovation and development, decision-making management and market development. At the same time, with the direction of socialized school running, it trains and trains chemical and practical technical talents to meet the high-end development needs of the petrochemical and chemical industry.
researchers are recording the response in the Shandong High-end Petrochemical Innovation and Entrepreneurship Community Laboratory. In order to promote the integration of "innovation chain" and "industrial chain", the community has gathered synergistic innovation force, and also actively promoted the cooperative research and development between Dalian University of Technology and Gangcheng Thermal. , the implementation of carbon dioxide replenishment and nitrogen production projects. The project device is the first set in the country, with an annual capture of 100,000 tons of carbon dioxide, which is mainly used for Shengli Oilfield oil displacement and storage. At present, Haike Ruilin Co., Ltd. has launched a pilot project on the methanol hydrogen production device, with a capture capacity of 150,000 tons/year.
took off formed a network of chains, and "chains" drive new advantages in industrial development. In order to promote the development of petrochemical industry clusters, the community has sorted out the bottleneck problems and "stuck neck" technical problems that restrict industrial innovation and development, and clarified the impact of high-quality industrial development on technological innovation. It focuses on solving the problem that a single element is unwilling to do it, cannot do it, and it is not cost-effective to do it.
"By organizing expert demonstrations and taking into account the actual situation in Shandong, especially in the Dongying area, we re-planned the carbon two, carbon three , carbon four and aromatic hydrocarbon industry chains, and sorted out 33 key technical problems from the four leading chains. To tackle key problems." Geng Shulin said, "At the same time, we have also selected a number of institutions such as the Dalian Institute of Chemistry, Chinese Academy of Sciences, China University of Petroleum, Dalian University of Technology, Qingdao University of Science and Technology, etc. as the main undertaking units involved in scientific research, giving full play to the community's 'beads' The role of forming a chain, forming a chain and forming a network."
builds and sorts out the industrial chain based on industrial clusters, and the community comprehensively sorts out the industrial chain according to the idea of "partition wall supply, upstream and downstream connection", and selects the lack of chain, extension of chain, and extension of chain. Projects with high technical level and high added value will be implemented and transformed. At the same time, the community has clarified the key direction of promotion, focusing on the development of high-performance resins and high-performance fibers.New chemical materials represented by dimensional and graphene materials, high-tech and high-value-added downstream chemical products represented by surfactants, additives, catalysts, , and special chemical products, including high-end general synthesis materials, high-performance plastics, high-end specialty chemicals, etc. The common volume of
is the cooperation between enterprises and scientific research institutes to "build bridges" and "chain" new advantages for the development of the industry. At present, the community is focusing on the development of high-end synthetic rubber by cooperation between Zhenhua New Materials, Haike Petrochemical and Dalian Institute of Chemical Technology of the Chinese Academy of Sciences according to the needs of enterprises, and Dongyue Petrochemical and Chinese Academy of Sciences to develop PTFE downstream special materials, Jingbo Petrochemical cooperated with Beijing University of Chemical Technology, Qingdao University of Science and Technology, and Dalian Institute of Chemistry, Chinese Academy of Sciences to develop polypropylene modified materials and bio-based elastomers, further extending the industrial chain, increasing the added value of traditional industries, and enhancing the enterprise market competitiveness, and promote the high-quality development of the industry.
has become a trend and has taken root, and scientific and technological achievements are no longer "shelved"
"relying on the talent advantages of the community, scientific research and innovation advantages, and through the accumulation of small experiments in the early stage, we expect to form a complete 10,000-ton grade polyterephthalic acid by the end of this year or next year. , 4-cyclohexanedimethyl ester (PCT) production process package." said Li You, deputy director of the Biochemical Division of Shandong Chemical Pilot Base.
Researchers are looking at PCT and its copolymer small-scale equipment
PCT is a high-end downstream product in the aromatic hydrocarbon industry chain with purified terephthalic acid (PTA) as the main raw material. At present, there are two product markets in the domestic aromatic hydrocarbon industry chain, PX and PTA. It has been in a saturated state, and now the PCT product has completed the pilot test and is about to form a complete process package for industrial production, which can effectively promote the aromatics product industry and value chain to the mid-to-high end. The
community takes the integration of the crude oil processing capacity of the existing local refining enterprises as the "oil head", improves the "incarnation" and "the tail" with the new large-scale project, accelerates the creation of an industrial chain of "the oil head turns into the high chemical tail", and develops scientific and technological achievements. Land transformation, so that scientific and technological achievements will no longer be "sheltered" -
signed a cooperation agreement on dual energy consumption control and dual carbon management with China Gas Industry Co., Ltd. on December 9 last year to accelerate the construction of "energy-industry-ecological synergy" ” carbon management system to help the chemical industry in Shandong Province achieve carbon peaking and carbon neutrality as soon as possible.
The pilot plant of Jiechuang atmospheric hydrogenation technology in the
community
and Dr. Wei Dongchu of Iperene Technology (Hangzhou) Co., Ltd. negotiated the pilot scale and industrialization of the polyolefin elastomer POE project, and further negotiated on this basis. To build a high-tech research center for polyolefins and fine chemicals, it is planned to introduce dozens of authoritative experts in the chemical industry at home and abroad to cooperate in the research and development of advanced linear alpha-olefins (LAO), liquid polyolefins (E-PO), polyethylene wax ( PE-Wax) technology and promote industrialization.
is negotiating with Shandong Haicheng Petrochemical Engineering Design Co., Ltd. maleic anhydride hydrogenation to succinic acid (anhydride), maleic anhydride hydrogenation to γ-butyrolactone , 1,4-butanediol technology development and industrialization , and plans to continue the in-depth development along the carbon tetramaleic anhydride industry chain in the future.
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At present, the community has settled in 8 pilot projects such as Dalian Institute of Chemistry, Chinese Academy of Sciences, China University of Petroleum, Qingdao University of Science and Technology, etc. More than 10 pilot projects such as high-performance polypropylene are being demonstrated to reduce foreign dependence.
(Reporter Jia Chongxiao)
Shandong Province High-end Petrochemical Innovation and Entrepreneurship Community
Five high-end pilot projects
1.PCT and its copolymer pilot project The PCT products of Eastman Company of the United States occupy the vast majority of the global market share. At present, there is no 100-ton production line for PCT and its copolymers in China. All PCT and its copolymer products need to be imported. The development of CHDM, the key monomer for domestic production of PCT and its copolymers, has made breakthroughs and solved the problem of the PCT industry. The problem of high raw material prices. The
community carried out pilot scale-up of PCT and its copolymers on a polyester plant, and receivedSet process parameters to form a complete process package. At present, the project has passed the pilot test, and the reaction has been scaled up step by step on the 10L and 30L polyester devices. A database of parameters such as reaction route, catalyst formula, process parameter conditions, and process flow has been established to prepare for the next scale-up experiment.
2. The key technology and application of furoic acid to prepare bio-based 2,5-furandicarboxylic acid (FDCA) It is the best compound to replace the important polyester monomer terephthalic acid (TPA), and it is recognized as a bio-based monomer with important commercial value. At present, my country is still in the technical reserve stage in terms of synthetic FDCA methods and processes. Aiming at the shortcomings of bulk polyester polyethylene terephthalate (PET), which is derived from petroleum-based and non-degradable, the
community starts from the non-food biomass furoic acid and aims at industrialization to efficiently prepare 2,5 -Furandicarboxylate, post-treatment through decolorization, acid-base neutralization, leaching, etc. to obtain polymer-grade FDCA, and gradually establish the first 300 tons/year 2,5-furandicarboxylic acid (FDCA) pilot production demonstration line in China . At present, the preparation of kilogram-scale FDCA has been realized, and the next step is to carry out scale-up experiments.
3. Pilot production of bio-based polyethylene 2,5-furandicarboxylate (PEF)
PEF is a renewable resource polymer material with excellent heat resistance, mechanical properties, solvent resistance and gas barrier properties. Barrier packaging materials, high-performance fibers and engineering plastics have broad application prospects and are expected to become new varieties of bulk polyester. The
community has formed a 10,000-ton PEF production process package based on the pilot production line and the corresponding polymerization process. At present, the small test and pilot test experiments have been completed, and the process parameters have been collected. The next step is the design and construction of the PEF pilot production line. Prepare.
4. Development of high-end rare earth cis-butadiene rubber complete sets of synthesis technology
rare earth cis-butadiene rubber is an important basic rubber type for high-performance tires recognized internationally, and it is the key to the upgrading of synthetic rubber products and the development of green tires in China. The
community mainly studies the establishment of a pilot plant for rare earth cis-butadiene rubber, conducts Nd-BR pilot process scale-up research, solves the problems of transmission, mass transfer and heat transfer of high-viscosity glue during the polymerization reaction, systematically optimizes process and component parameters, and forms High-end rare earth butadiene rubber process package with independent intellectual property rights. At present,
has completed the small test and scale-up experiments, the relevant equipment procurement has been completed, and the pilot scale-up production line is under construction.
5. Carbon Materials Research Center Project
The main purpose of carrying out the Carbon Materials Research Center project is to use heavy aromatic hydrocarbons as raw materials to produce high-performance pitch -based carbon fiber products urgently needed by the country, to provide high-quality carbon materials for national strategic development, and to improve corporate competition. force to promote the development of my country's carbon fiber upstream and downstream industries.
The pilot-scale equipment
of China University of Petroleum (Beijing) Carbon Materials Research Center in the community is led by the community, and the research team of the State Key Laboratory of Heavy Oil, China University of Petroleum (Beijing) extends the research work to the front line of enterprises, combining the results Transform and carry out project construction , and establish special achievement research institutions. The project adopts the processing route of "supercritical extraction of heavy aromatic hydrocarbons + desulfurization and refining of rich aromatic hydrocarbons + mesophase pitch polymerization + melt spinning + oxidative carbonization", and is currently in the stage of pilot-scale optimization of process parameters.
(reporter Jia Zhongxiao correspondent Guo Feng)
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